Pyridine Hydrochloride 吡啶盐酸盐
CAS 628-13-7 MFCD00012802
化学结构图
SMILES: Cl.c1ccncc1
化学属性
| Mol. Formula | C5H6ClN |
|---|---|
| Mol. Weight | 115.56 |
| Density | 1.0 |
| Boiling Point | 222-224 °C at 760 mmHg |
| Melting Point | 145-147 °C |
| TSCA | Yes |
| Solubility | 85 G/100 ML |
| Stability | 易吸潮 |
| Flash Point | 222-224°C |
别名和识别编码
| Chemical Name | Pyridine Hydrochloride |
|---|---|
| CAS Number | 628-13-7 |
| Synonym | Pyridine (hydrochloride) {LY} Pyridine (hydrochloride) {} {LY} Pyridine (hydrochloride) {} {} {LY} Pyridine (hydrochloride) {} {} {} {LY} Pyridine (hydrochloride) {} {} {} {} {LY} Pyridine (hydrochloride) {} {} {} {} {} {LY} Pyridine (hydrochloride) {} {} {} {} {} {} {LY} Pyridine (hydrochloride) {} {} {} {} {} {} {} {LY} Pyridine (hydrochloride) {} {} {} {} {} {} {} {} {LY} Pyridine (hydrochloride) {} {} {} {} {} {} {} {} {} {LY} Pyridine (hydrochloride) {} {} {} {} {} {} {} {} {} {} {LY} Pyridine (hydrochloride) {} {} {} {} {} {} {} {} {} {} {} {LY} Pyridine (hydrochloride) {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} Pyridine (hydrochloride) {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} Pyridine (hydrochloride) {} {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} Pyridine (hydrochloride) {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} { {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} Pyridi |
| MDL Number | MFCD00012802 |
| EC Number | 211-027-4 |
| Beilstein Registry Number | 3615340 |
| PubChem Substance ID | 87557963 |
| Reaxys-RN | 3615340 |
| Chemical Name Translation | 吡啶盐酸盐 |
| Wiswesser Line Notation | T6NJ &GH |
| LabNetwork Molecule ID | LN02210656 |
| Canonical SMILES | Cl.N1=CC=CC=C1 |
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分类
- {uni_hamburg} no charge; nitrogen heterocycle; 6RingOnly; 6ring; 2fragments; ionic
- Heterocycles
- Miscellaneous Reagents
- Intermediates
- Aromatics
- {SNA} Building Blocks, C5, Chemical Synthesis, Heterocyclic Building Blocks, Pyridines
产品应用
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相关文献及参考
- {
- Demethylation of methyl aryl ethers can also be carried out under solvent-free conditions with microwave irradiation: J. Chem. Res. (Synop.), 394 (1999).
- Short: III/20a
- Short: IV/1a
- Cleaves N-trityl groups from histidine residues in peptide synthesis: Tetrahedron Lett., 28, 6031 (1987).
- Mild acid catalyst, e.g. in the formation of acetals with ethylene glycol: J. Org. Chem., 31, 26 (1966), or 1,3-propanediol: Bull. Soc. Chim. Fr., 2287 (1972); and in the Fischer indole synthesis for acid-sensitive substrates: Synthesis, 645 (1977).
- Epoxides at ambient temperature in chloroform give chlorohydrins: Synth. Commun., 11, 287 (1981).
- Beilstein:20(5)5,160
- Egyed, J. et al.: Bull. Soc. Chim. Fra., 11, 3014 (1973); Li, Y. et al.: Wuli HUa. Xueb., 14, 1048 (1998);
- In DMF, has been used for the conversion of alkyl tosylates to chlorides at room temperature: J. Am. Chem. Soc., 80, 2726 (1958).
- Classical reagent for cleavage of aryl methyl ethers at 200-220 o : Ber ., 75, 445 (1942), avoiding the strongly acidic or basic conditions of some alternative methods; see, e.g.: J. Org. Chem., 27, 4660 (1962):
- Short: II/2
安全信息
GHS Symbol
- S26 In case of contact with eyes, rinse immediately with plenty of water and seek medical advice 眼睛接触后，立即用大量水冲洗并征求医生意见；
- S36 Wear suitable protective clothing 穿戴适当的防护服；
- R20/21/22 Harmful by inhalation, in contact with skin and if swallowed 吸入、皮肤接触和不慎吞咽有害
- R22 Harmful if swallowed 吞咽有害
- R36/37/38 Irritating to eyes, respiratory system and skin 对眼睛、呼吸系统和皮肤有刺激性
- P261 Avoid breathing dust/fume/gas/mist/vapours/spray. 避免吸入粉尘/烟/气体/烟雾/蒸汽/喷雾。
- P264 Wash hands thoroughly after handling. 处理后要彻底洗净双手。
- P270 Do not eat, drink or smoke when using this product. 使用本产品时不要吃东西，喝水或吸烟。
- P280 Wear protective gloves/protective clothing/eye protection/face protection. 戴防护手套/防护服/眼睛的保护物/面部保护物。
- P301+P312+P330
- P302+P352+P332+P313+P362+P364
- P305+P351+P338
- P305+P351+P338+P337+P313
- P332+P313
- P362 Take off contaminated clothing and wash before reuse. 脱掉污染的衣服，清洗后方可重新使用
- P501 Dispose of contents/container to..… 处理内容物/容器.....
- H302 Harmful if swallowed 吞食有害
- H315 Causes skin irritation 会刺激皮肤
- H335 May cause respiratory irritation 可能导致呼吸道刺激
- H302+H332
- H319 Causes serious eye irritation 严重刺激眼睛
- H332 Harmful if inhaled 吸入有害
TYPE OF TEST : LD50 - Lethal dose, 50 percent kill ROUTE OF EXPOSURE : Oral SPECIES OBSERVED : Rodent - rat DOSE/DURATION : 1600 mg/kg TOXIC EFFECTS : Details of toxic effects not reported other than lethal dose value REFERENCE : KODAK* Kodak Company Reports. (343 State St., Rochester, NY 14650) Volume(issue)/page/year: 21MAY1971
TYPE OF TEST : LD50 - Lethal dose, 50 percent kill ROUTE OF EXPOSURE : Administration onto the skin SPECIES OBSERVED : Rodent - guinea pig DOSE/DURATION : 2500 uL/kg TOXIC EFFECTS : Details of toxic effects not reported other than lethal dose value REFERENCE : KODAK* Kodak Company Reports. (343 State St., Rochester, NY 14650) Volume(issue)/page/year: 21MAY1971
TYPE OF TEST : LD50 - Lethal dose, 50 percent kill ROUTE OF EXPOSURE : Intraperitoneal SPECIES OBSERVED : Rodent - rat DOSE/DURATION : 800 mg/kg TOXIC EFFECTS : Details of toxic effects not reported other than lethal dose value REFERENCE : KODAK* Kodak Company Reports. (343 State St., Rochester, NY 14650) Volume(issue)/page/year: 21MAY1971
其他信息
- MOL 文件:628-13-7.mol
- Sigma Aldrich:628-13-7(sigmaaldrich)
- MSDS 信息:Pyridine hydrochloride(628-13-7).msds
- F:3-10
- 遇空气极易吸湿并呈水样，有吡啶臭味。水中溶解度: 85G/100G水
- TCI Shanghai:吡啶盐酸盐 Pyridine Hydrochloride,>;98.0%(T)(628-13-7)
- Acros Organics:吡啶盐酸盐 Pyridine hydrochloride, pure, 98%(628-13-7)
- 用途一:用作医药中间体
- 吡啶盐酸盐价格(试剂级):更新日期 产品编号 产品名称 包装 价格 2011/08/23 30160224 吡啶盐酸盐;盐酸吡啶 25g 63元 2011/04/16 P1637 吡啶盐酸盐 Pyridine Hydrochloride 500G 1190元 2011/04/16 P1637 吡啶盐酸盐 Pyridine Hydrochloride 25G 196元
- 外观性质:白色结晶性粉末，遇空气极易吸湿并呈水样，有吡啶臭味。水中溶解度: 85G/100G水沸点:222-224℃熔点:147℃
- Alfa Aesar:嘧啶盐酸盐,98% Pyridine hydrochloride, 98%(628-13-7)
- 海关编码:29333100
- 下游产品:西伯尔链接剂
- 敏感性:Hygroscopic
