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分类

• {SNA} Building Blocks, Carbonyl Compounds, Chemical Synthesis, Hydrazides, Organic Building Blocks
• {uni_hamburg} no charge; amide; 1fragment
• Building Blocks, Carbonyl Compounds, Chemical Synthesis, Hydrazides, Organic Building Blocks

相关文献及参考

• Beil. 2 ,IV,435
• Aldrich MSDS 1 , 7:A / Corp MSDS 1 (1), 18:B / FT-IR 1 (1), 768:B / FT-IR 2 (1), 1294:C / FT-NMR 1 (1), 1254:C / IR-Spectra (3), 448:H / IR-Spectra (2), 396:H / NMR-Reference 2 (1), 645:B / RegBook 1 (1), 903:B / Sax 6 , 112 / Sigma FT-IR 1 (2), 231:C / Structure Index 1 , 138:A:8
• Short: III/20a Title: Nuclear Quadrupole Resonance Spectroscopy Data: Nuclei D ... Cl Author: Chihara, H.; Nakamura, N. Editor: Hellwege, K.-H.; Hellwege, A.M. Source: Landolt-Börnstein, New Series Volume: III/20a Year: 1988 Keyword: NQR ISBN: 3-540-18161-X ISBN: 978-3-540-18161-3 Internet Resource: DOI:10.1007/b31153 RefComment: IX,677 pages. Hardcover Abstract: Nuclear Quadrupole Resonance Spectroscopy has become a standard method for structural research in molecular and solid state physics as well as for different branches of chemistry. The volumes cover data for more than 8,000 substances in the solid state. Data for free molecules have been published in volumes II/14 and II/15 of the New Series. The tables are arranged according to the atomic number of the elements.
• Short: III/35B Title: Nuclear Magnetic Resonance (NMR) Data: Chemical Shifts and Coupling Constants for Fluorine-19 and Nitrogen-15 Author: Balasubramanian, M.; Gupta, R.R.; Jain, M.; Perumal, S. Editor: Gupta, R.R.; Lechner, M.D. Source: Landolt-Börnstein, New Series Volume: III/35B Year: 1998 ISBN: 3-540-63275-1 ISBN: 978-3-540-63275-7 Internet Resource: DOI:10.1007/b55685 RefComment: VII, 242 pages. With CD-ROM. Hardcover Abstract: This volume provides a comprehensive and evaluated compilation of nuclear magnetic resonance data. Chemical shifts and coupling constants of boron-11 and phosphorus-31 (subvol. A), fluorine-19 and nitrogen-15 (subvol. B), hydrogen-1 (subvol. C), and carbon-13 (subvol. D) compounds are tabulated together with the gross- and structure formulas and the most readily available

安全信息

GHS Symbol

TYPE OF TEST            : LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE       : Intraperitoneal
SPECIES OBSERVED        : Rodent - mouse
DOSE/DURATION           : 153 mg/kg
TOXIC EFFECTS :
   Behavioral - convulsions or effect on seizure threshold
REFERENCE :
   JPETAB Journal of Pharmacology and Experimental Therapeutics.  (Williams &
   Wilkins Co., 428 E. Preston St., Baltimore, MD 21202)  V.1-    1909/10-
   Volume(issue)/page/year: 122,110,1958

TYPE OF TEST            : LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE       : Oral
SPECIES OBSERVED        : Bird - wild bird species
DOSE/DURATION           : 42200 ug/kg
TOXIC EFFECTS :
   Details of toxic effects not reported other than lethal dose value
REFERENCE :
   AECTCV Archives of Environmental Contamination and Toxicology.
   (Springer-Verlag New York, Inc., Service Center, 44 Hartz Way, Secaucus, NJ
   070944)  V.1-    1973-  Volume(issue)/page/year: 12,355,1983

TYPE OF TEST            : LDLo - Lowest published lethal dose
ROUTE OF EXPOSURE       : Subcutaneous
SPECIES OBSERVED        : Rodent - rabbit
DOSE/DURATION           : 116 mg/kg
TOXIC EFFECTS :
   Endocrine - hypoglycemia
REFERENCE :
   JPETAB Journal of Pharmacology and Experimental Therapeutics.  (Williams &
   Wilkins Co., 428 E. Preston St., Baltimore, MD 21202)  V.1-    1909/10-
   Volume(issue)/page/year: 30,87,1927

TYPE OF TEST            : Mutation in microorganisms
TEST SYSTEM             : Bacteria - Salmonella typhimurium
DOSE/DURATION           : 500 ug/plate
REFERENCE :
   IJEBA6 Indian Journal of Experimental Biology.  (Publications & Information
   Directorate, CSIR, Hillside Rd., New Delhi 110 012, India)  V.1-    1963-
   Volume(issue)/page/year: 19,939,1981

TYPE OF TEST            : Mutation in microorganisms
TEST SYSTEM             : Microorganism - not otherwise specified
DOSE/DURATION           : 70 mg/L
REFERENCE :
   MUREAV Mutation Research.  (Elsevier Science Pub. B.V., POB 211, 1000 AE
   Amsterdam, Netherlands) V.1-    1964-  Volume(issue)/page/year: 173,233,1986

TYPE OF TEST            : DNA inhibition
ROUTE OF EXPOSURE       : Intraperitoneal
TEST SYSTEM             : Rodent - mouse
DOSE/DURATION           : 150 mg/kg
REFERENCE :
   IJEBA6 Indian Journal of Experimental Biology.  (Publications & Information
   Directorate, CSIR, Hillside Rd., New Delhi 110 012, India)  V.1-    1963-
   Volume(issue)/page/year: 19,939,1981

TYPE OF TEST            : Micronucleus test
ROUTE OF EXPOSURE       : Intraperitoneal
TEST SYSTEM             : Rodent - mouse
DOSE/DURATION           : 120 mg/kg
REFERENCE :
   CALEDQ Cancer Letters (Shannon, Ireland).  (Elsevier Scientific Pub. Ireland
   Ltd., POB 85, Limerick, Ireland)  V.1-    1975- Volume(issue)/page/year:
   23,235,1984

其他信息

• 下游产品:2-巯基-5-甲基-1,3,4-噻二唑 --> 5-甲基-1,3,4-噁二唑酮
• 用途三:乙酰肼是重要的有机合成中间体，在农药上是杀虫剂吡嗪酮的中间体，也是除草剂苯嗪草酮的中间体，在医药上主要用于合成硝呋隆(nifuratrone)。
• 用途二:乙酰肼是除草剂苯嗪草酮的中间体。
• Acros Organics:乙酸肼 Acethydrazide, 95%(1068-57-1)
• MSDS 信息:Acethydrazide(1068-57-1).msds
• 用途一:用作有机合成中间体
• 方法二:其制备方法是用乙酸乙酯与水合肼在Al 2 O 3 存在下，反应得到乙酰肼。反应方程式：CH 3 COOC 2 H 5 +NH 2 NH 2 ·H 2 O→CH 3 CONHNH 2 +C 2 H 5 OH
• 方法一:其制备方法是在反应器中加入乙酸乙酯与水合肼，加热回流数小时，然后减压蒸馏得成品。 CH 3 COOC 2 H 5 +NH 2 NH 2 ·H 2 O→CH 3 CONHNH 2 +C 2 H 5 OH
• F:3-8-10
• Alfa Aesar:乙酰肼,96% Acetic hydrazide, 96%(1068-57-1)
• Sigma Aldrich:1068-57-1(sigmaaldrich)
• TCI Shanghai:乙酰肼 Acetohydrazide,>;98.0%(T)(1068-57-1)
• 乙酰肼价格(试剂级):更新日期 产品编号 产品名称 包装 价格 2014/06/02 A0789 乙酰肼 Acetohydrazide 25G 378元 2014/06/02 A0789 乙酰肼 Acetohydrazide 500G 3120元 2010/06/21 102350250 乙酰肼 Acethydrazide 95% 25 GR 685元
• 敏感性:Hygroscopic
• 海关编码:29280090
• 所属类别二:农药中间体: 除草剂中间体: 除草剂中间体
• MOL 文件:1068-57-1.mol
• 图谱信息:乙酰肼(1068-57-1)Raman光谱 乙酰肼(1068-57-1)红外图谱(IR1) 乙酰肼(1068-57-1)核磁图( 1 HNMR) 乙酰肼(1068-57-1)核磁图( 13 CNMR) 乙酰肼(1068-57-1)质谱(MS) 乙酰肼(1068-57-1)红外图谱(IR2)
• 所属类别一:农药中间体: 杀虫剂中间体: 其他杀虫剂
• 上游原料:2-甲基-2-丙烯酸-2-丁氧基乙酯